University of Oulu

Khallok, H., Ojala, S., Ezzahmouly, M. et al. J Aust Ceram Soc (2019) 55: 611. https://doi.org/10.1007/s41779-018-0269-1

Porous foams based hydroxyapatite prepared by direct foaming method using egg white as a pore promoter

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Author: Khallok, Hamza1; Ojala, Satu2; Ezzahmouly, Manal1;
Organizations: 1Electrochemical and Biomaterials Team, Chemistry Department, Faculty of Sciences, University Chouaib Doukkali, El Jadida, Morocco
2Environmental and Chemical Engineering, Faculty of Technology, University of Oulu, Oulu, Finland
Format: article
Version: accepted version
Access: embargoed
Persistent link: http://urn.fi/urn:nbn:fi-fe201903138764
Language: English
Published: Springer Nature, 2019
Publish Date: 2019-10-01
Description:

Abstract

Stoichiometric hydroxyapatite (Ca₁₀(PO)₆(OH)₂, HAP) foams have been produced. The porous parts were prepared from a calcined HAP powder and egg white as a bio and non-toxic pore promoter. The colloidal slurry was prepared, poured into cylindrical molds, dried, unmolded, and sintered at 1200 °C. The effects of the concentration of the solid loading, of the dispersing agent, and the foaming agent on the ceramic preparation were examined. X-ray diffraction (XRD) and Fourier transform infrared (FTIR) were used to evaluate the composition and the structure of the sintered HAP ceramics. Scanning electron microscopy (SEM) was used for microstructural analysis. The XRD analysis of the porous parts, prepared under optimized conditions, showed the presence of crystallized HAP (JCPDS 9-432) as a single phase. SEM images showed existence of open and interconnected micro and macropores in the ceramics. The use of the egg white protein as pore former provides a total porosity of 86 vol% and a foam-structure that allows to a microporous wall.

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Series: Journal of the Australian Ceramic Society
ISSN: 2510-1560
ISSN-E: 2510-1579
ISSN-L: 2510-1560
Volume: 55
Issue: 2
Pages: 611 - 619
DOI: 10.1007/s41779-018-0269-1
OADOI: https://oadoi.org/10.1007/s41779-018-0269-1
Type of Publication: A1 Journal article – refereed
Field of Science: 218 Environmental engineering
Subjects:
Copyright information: © Australian Ceramic Society 2018. This is a post-peer-review, pre-copyedit version of an article published in J Aust Ceram Soc. The final authenticated version is available online at: https://doi.org/10.1007/s41779-018-0269-1.