University of Oulu

Patnamsetty, M.; Ghosh, S.; Somani, M. C.; & Peura, P. (2023). Dynamic softening kinetics of Al0.3CoCrFeNi high-entropy alloy during high temperature compression and its correlation with the evolving microstructure and micro-texture. In Materials Characterization (Vol. 197, p. 112693). Elsevier BV. https://doi.org/10.1016/j.matchar.2023.112693

Dynamic softening kinetics of Al0.3CoCrFeNi high-entropy alloy during high temperature compression and its correlation with the evolving microstructure and micro-texture

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Author: Patnamsetty, Madan1; Ghosh, Sumit2; Somani, Mahesh C.2;
Organizations: 1Materials Science and Environmental Engineering, Tampere University, 33720 Tampere, Finland
2Materials and Mechanical Engineering, Centre for Advanced Steels Research, University of Oulu, 90014, Finland
Format: article
Version: published version
Access: open
Online Access: PDF Full Text (PDF, 33.2 MB)
Persistent link: http://urn.fi/urn:nbn:fi-fe20230825107148
Language: English
Published: Elsevier, 2023
Publish Date: 2023-08-25
Description:

Abstract

To establish the characteristics and kinetics of dynamic softening in a Al0.3CoCrFeNi high–entropy alloy (HEA), isothermal compression tests were carried out in a suitable temperature range of 1273–1423 K at 10-2 and 10-1 s-1 in accord with our previous study. It was found that the discontinuous dynamic recrystallization (DRX) was the dominant microstructural reconstitution mechanism. The conditions of critical stress/strain for the onset of dynamic recrystallization were determined using the Poliak–Jonas analytical criterion. Further, a kinetic model was established based on the Avrami-type function in order to be able to predict the volume fraction of DRX. The DRX volume fraction expectedly increased with strain. The microstructural investigation of the isothermally compressed specimens revealed a good agreement with the proposed DRX kinetics model and validated its accuracy. Additionally, the evolution of DRX with strain was characterized by interrupting the test carried out at 1323 K/10-1 s-1 at different strains. The progress of DRX evolving as increased formation of new recrystallized grains further corroborated the predictions of the kinetic model. The micro-texture analysis revealed random texture in the recrystallized grains, whereas the unrecrystallized grains had shown their preferred orientation towards the <101> fiber texture.

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Series: Materials characterization
ISSN: 1044-5803
ISSN-E: 1873-4189
ISSN-L: 1044-5803
Volume: 197
Article number: 112693
DOI: 10.1016/j.matchar.2023.112693
OADOI: https://oadoi.org/10.1016/j.matchar.2023.112693
Type of Publication: A1 Journal article – refereed
Field of Science: 216 Materials engineering
Subjects:
Funding: Authors acknowledge TUNI Foundation as a part of Tampere university's graduate school, Ella and Georg Ehrnrooth foundation, and Walter Ahlström foundation for the financial support.
Dataset Reference: Original data will be made available by the authors on request.
Copyright information: © 2023 The Authors. Published by Elsevier Inc. This is an open access article under the CC BY license (http://creativecommons.org/licenses/by/4.0/).
  https://creativecommons.org/licenses/by/4.0/